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El diagrama de difracción de la muestra DET1 presenta un total de 56 máximos, situados en las siguientes posiciones [ver tabla en modo texto]:
|
Máximo |
Posición (2q) |
Posición (d) |
Intensidad (cuentas) |
Intensidad (%) |
Fondo continuo (cuentas) |
|
1 |
16.23536 |
5.4548 |
276.01456 |
14.6 |
82.40831 |
|
2 |
16.37049 |
5.4100 |
348.07834 |
18.5 |
83.40407 |
|
3 |
16.85695 |
5.2550 |
137.88007 |
7.3 |
80.90968 |
|
4 |
18.82740 |
4.7092 |
708.91656 |
37.6 |
119.92832 |
|
5 |
19.02644 |
4.6604 |
843.47540 |
44.7 |
124.49851 |
|
6 |
19.37262 |
4.5779 |
643.66058 |
34.1 |
129.61267 |
|
7 |
19.80690 |
4.4785 |
248.53320 |
13.2 |
129.05377 |
|
8 |
23.14613 |
3.8394 |
235.08383 |
12.5 |
164.16278 |
|
9 |
23.57747 |
3.7701 |
250.13013 |
13.3 |
159.63838 |
|
10 |
23.75408 |
3.7425 |
295.53497 |
15.7 |
149.80453 |
|
11 |
24.08393 |
3.6920 |
258.46811 |
13.7 |
128.09605 |
|
12 |
24.78634 |
3.5889 |
322.86572 |
17.1 |
113.34715 |
|
13 |
25.98874 |
3.4255 |
255.04941 |
13.5 |
124.63453 |
|
14 |
26.98212 |
3.3016 |
195.82159 |
10.4 |
136.97409 |
|
15 |
27.64931 |
3.2235 |
215.44565 |
11.4 |
128.02286 |
|
16 |
28.02936 |
3.1806 |
786.37659 |
41.7 |
117.89200 |
|
17 |
28.99866 |
3.0765 |
594.75128 |
31.6 |
133.71161 |
|
18 |
29.29572 |
3.0459 |
252.07375 |
13.4 |
146.67136 |
|
19 |
29.63150 |
3.0122 |
472.45944 |
25.1 |
158.82230 |
|
20 |
30.12908 |
2.9636 |
839.39453 |
44.5 |
163.17368 |
|
21 |
31.07012 |
2.8759 |
151.29410 |
8.0 |
124.24613 |
|
22 |
31.31845 |
2.8537 |
164.68941 |
8.7 |
136.86063 |
|
23 |
31.79365 |
2.8121 |
301.31918 |
16.0 |
188.36015 |
|
24 |
32.11938 |
2.7843 |
1884.88086 |
100.0 |
229.38753 |
|
25 |
32.50620 |
2.7521 |
276.90045 |
14.7 |
267.39474 |
|
26 |
32.75849 |
2.7314 |
300.95435 |
16.0 |
280.71899 |
|
27 |
33.10686 |
2.7035 |
880.98840 |
46.7 |
285.76648 |
|
28 |
33.22287 |
2.6943 |
876.32074 |
46.5 |
284.52124 |
|
29 |
33.83809 |
2.6467 |
1546.67505 |
82.1 |
259.91202 |
|
30 |
34.12952 |
2.6248 |
1004.86823 |
53.3 |
241.25745 |
|
31 |
34.52701 |
2.5955 |
1086.15247 |
57.6 |
213.28975 |
|
32 |
35.20749 |
2.5469 |
479.47208 |
25.4 |
171.16161 |
|
33 |
35.85091 |
2.5026 |
415.39011 |
22.0 |
140.00121 |
|
34 |
36.51879 |
2.4584 |
288.52139 |
15.3 |
132.14864 |
|
35 |
37.11826 |
2.4200 |
405.96548 |
21.5 |
152.25586 |
|
36 |
37.99216 |
2.3663 |
946.10687 |
50.2 |
158.28033 |
|
37 |
38.59714 |
2.3306 |
665.79272 |
35.3 |
136.31686 |
|
38 |
39.31094 |
2.2899 |
152.31949 |
8.1 |
116.35147 |
|
39 |
39.92615 |
2.2561 |
494.58807 |
26.2 |
120.50457 |
|
40 |
40.73930 |
2.2129 |
199.05693 |
10.6 |
129.45148 |
|
41 |
41.09549 |
2.1945 |
361.71448 |
19.2 |
132.49690 |
|
42 |
41.45499 |
2.1763 |
403.22824 |
21.4 |
135.74754 |
|
43 |
42.15551 |
2.1418 |
241.27655 |
12.8 |
140.76085 |
|
44 |
43.99986 |
2.0562 |
179.96486 |
9.5 |
133.41869 |
|
45 |
44.80464 |
2.0211 |
362.94705 |
19.3 |
124.59399 |
|
46 |
45.43668 |
1.9944 |
205.66417 |
10.9 |
120.35703 |
|
47 |
46.48840 |
1.9517 |
309.75577 |
16.4 |
147.94608 |
|
48 |
46.99877 |
1.9317 |
239.62711 |
12.7 |
176.05916 |
|
49 |
47.54037 |
1.9110 |
306.56070 |
16.3 |
191.56331 |
|
50 |
48.22984 |
1.8852 |
436.31836 |
23.1 |
199.20357 |
|
51 |
48.76358 |
1.8658 |
625.01239 |
33.2 |
198.14525 |
|
52 |
49.38618 |
1.8438 |
297.10342 |
15.8 |
166.33304 |
|
53 |
50.77636 |
1.7965 |
303.18964 |
16.1 |
130.33578 |
|
54 |
52.17138 |
1.7517 |
271.05209 |
14.4 |
109.43363 |
|
55 |
53.54843 |
1.7099 |
276.58496 |
14.7 |
184.35916 |
|
56 |
54.54562 |
1.6809 |
460.84845 |
24.4 |
139.45029 |
Para generar un fichero de entrada a los programas de asignación de índices de Miller a los máximos de difracción (DICVOL91 y TREOR90), guarda en tu ordenador y modifica adecuadamente los ficheros ejemplo ejemTRE.inp y ejemDIC.dic.
